Determination of the Crystallographic Parameters of 2,2- Diphenyl-[1,3,2]Dithiagermole-4,5-Dicarbonitrile by Using X-Ray Powder Diffraction
Öz
Using X-ray powder diffraction technique, diffraction pattern of compound of 2,2-diphenyl-[1,3,2]dithiagermole-4,5-dicarbonitrile was recorded. Profiting pattern, the crystal lattice and crystallographic parameters of the title compound were determined using analytic method and ITO computer program. According to the analytical method, the crystal system is monoclinic and unit cell parameters are; a=15.7202 Å, b=14.0053 Å, c=15.2543 Å, β=105.265º. Using ITO program, the type of crystal lattice was found as monoclinic and parameters of unit cell are a=15.7630 Å, b=14.0094 Å, c=15.3186 Å, β=105.451º. The results of the program are in agreement with those of analytical method.
Anahtar Kelimeler
X-ray powder diffraction 2 2-diphenyl-[1 3 2]dithiagermole-4 5-dicarbonitrile Crystallographic parameters
Kaynakça
- Eye, R. D., Wait, E., Phil, D., ‘‘X-Ray Powder Photography in Inorganic Chemistry’’, Butterworths Scientific Publications, London, 70- 97 (1960).
- Akkurt, M., Öztürk, S., Kök, T., Fun, H. K., “2,2- diphenyl-1,3,2-dithiagermole-4,5-dicarbonitrile”, Acta Cryst., E59, 664-665 (2003).
- J. W., Visser, ‘‘A Fully Automatic Program for Finding the Unit Cell from Powder Data’’, J.Appl. Cryst., 2: 89-95 (1969).
- H. M., Haendler, W. A., Cooney ‘‘Computer Determination of Unit-Cell from Powder- Difraction Data’’, Acta Cryst. ,16: 1243-1248 (1963).
- User’s Manual, “Diffrac Plus WIN-INDEX Professional Powder Indexing”, Bruker AXS, Karlsruhe, 7-33, (1998).
- Azaroff, V., Buerger, M., ‘‘The Powder Method in X-Ray Crystallography’’, Mc. Graw-Hill Book Company, New York, 82-91 (1958).
Öz
Kaynakça
- Eye, R. D., Wait, E., Phil, D., ‘‘X-Ray Powder Photography in Inorganic Chemistry’’, Butterworths Scientific Publications, London, 70- 97 (1960).
- Akkurt, M., Öztürk, S., Kök, T., Fun, H. K., “2,2- diphenyl-1,3,2-dithiagermole-4,5-dicarbonitrile”, Acta Cryst., E59, 664-665 (2003).
- J. W., Visser, ‘‘A Fully Automatic Program for Finding the Unit Cell from Powder Data’’, J.Appl. Cryst., 2: 89-95 (1969).
- H. M., Haendler, W. A., Cooney ‘‘Computer Determination of Unit-Cell from Powder- Difraction Data’’, Acta Cryst. ,16: 1243-1248 (1963).
- User’s Manual, “Diffrac Plus WIN-INDEX Professional Powder Indexing”, Bruker AXS, Karlsruhe, 7-33, (1998).
- Azaroff, V., Buerger, M., ‘‘The Powder Method in X-Ray Crystallography’’, Mc. Graw-Hill Book Company, New York, 82-91 (1958).
Ayrıntılar
| Birincil Dil | İngilizce |
|---|---|
| Konular | Mühendislik |
| Bölüm | Physics |
| Yazarlar | |
| Yayımlanma Tarihi | 28 Mart 2010 |
| Yayımlandığı Sayı | Yıl 2007 Cilt: 20 Sayı: 4 |